任翌劼, 黄启玉, 朱方达, 王文达. 高含蜡胶凝油的蜡晶显微特性[J]. 油气储运, 2017, 36(4): 409-415. DOI: 10.6047/j.issn.1000-8241.2017.04.009
引用本文: 任翌劼, 黄启玉, 朱方达, 王文达. 高含蜡胶凝油的蜡晶显微特性[J]. 油气储运, 2017, 36(4): 409-415. DOI: 10.6047/j.issn.1000-8241.2017.04.009
REN Yijie, HUANG Qiyu, WANG Fangda, WANG Wenda. Microscopic characteristics of wax crystal in gelling oil with high wax content[J]. Oil & Gas Storage and Transportation, 2017, 36(4): 409-415. DOI: 10.6047/j.issn.1000-8241.2017.04.009
Citation: REN Yijie, HUANG Qiyu, WANG Fangda, WANG Wenda. Microscopic characteristics of wax crystal in gelling oil with high wax content[J]. Oil & Gas Storage and Transportation, 2017, 36(4): 409-415. DOI: 10.6047/j.issn.1000-8241.2017.04.009

高含蜡胶凝油的蜡晶显微特性

Microscopic characteristics of wax crystal in gelling oil with high wax content

  • 摘要: 为了研究管道蜡沉积物蜡晶形态与结构强度的关系,室内制备了不同含蜡比例的胶凝油,模拟现场管道蜡沉积物。借助软件Image J对不同实验条件下拍摄的胶凝油蜡晶显微图像进行处理,确定40 ℃是该实验蜡晶显微图像的拍摄温度。结果表明:随着胶凝油含蜡量的增大,蜡晶颗粒数与面积分数增大,蜡晶圆度也增大,但长径比减小,且长径比集中分布在1.50~2.00的范围内,表明大部分蜡晶形态呈长棒状。此外,结合胶凝油的屈服应力特性测试,分析蜡晶形态与其结构强度之间的关系:随着含蜡量的增大,蜡晶的边界盒维数增大,屈服应力也随之增大。由此可知:胶凝油内部的蜡晶形态差异是导致其结构强度随含蜡量变化的根本原因,研究结果为今后原油管道的清管工作提供了技术支持。

     

    Abstract: In order to investigate the relation between wax crystal morphology of wax deposit in pipelines and its structural strength, gelling oil with different wax contents was prepared in the lab to simulate wax deposits in the field pipelines. Then, the wax crystal microscopic images which were taken in different experimental conditions were processed by the Image J software. And it is confirmed that these micro images were taken at the temperature of 40 ℃. It is shown that with the increasing of wax content in gelling oil, the particle quantity, area fraction and roundness of wax crystal increase and its aspect ratio decreases. The aspect ratio is mainly distributed in the range of 1.50-2.00, indicating that the wax crystals are mostly in the shape of long rod. Finally, the relation between wax crystal morphology and its structural strength was analyzed with yield stress behavior test of gelling oil. And it is shown that with the increasing of wax content, the bounding fractal dimension and yield stress of wax crystal increase. It is concluded that the morphologic difference of wax crystal inside gelling oil is the fundamental reason why the structural strength of wax crystal varies with the wax content. The research results provide technical support for oil pipeline pigging in the future.

     

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